N,N-Diisopropylethylamine (DIPEA)


N,N-Diisopropylethylamine (DIPEA)

CAS 7087-68-5

Hünig’s Base · C₈H₁₉N · MW 129.24

Product Overview

N,N-Diisopropylethylamine (DIPEA), also known as Hünig’s Base, is a highly hindered tertiary amine widely used as a non-nucleophilic base in organic synthesis. With its excellent solubility in organic solvents and minimal nucleophilicity, DIPEA is the preferred base for peptide coupling, alkylation reactions, enolboration, and palladium-catalyzed alkoxycarbonylation. Our product achieves 99.97% purity (GC) with water content below 0.01%, exceeding standard pharmaceutical-grade specifications.

Technical Specifications

CAS Number 7087-68-5
Molecular Formula C₈H₁₉N
Molecular Weight 129.24 g/mol
Appearance Colorless clear liquid
Purity (GC) ≥99.70% (Actual: 99.97%)
Diisopropylamine ≤0.05% (Not Detected)
Any Single Impurity ≤0.10%
Water Content (KF) ≤0.05% (Actual: 0.01%)
Color (APHA) ≤25
Boiling Point 127 °C
Density 0.742 g/mL at 25 °C

Batch QC Data (Lot 26-05-08)

99.97%
Purity (GC)
0.01%
Water Content
ND
Diisopropylamine
150 kg
Batch Size

Applications

🧬 Peptide Synthesis

Preferred non-nucleophilic base for solid-phase and solution-phase peptide coupling. Compatible with HBTU, HATU, and carbodiimide activation methods. The extreme steric hindrance ensures no racemization of sensitive amino acids.

⚗️ Alkylation & Acylation

Ideal for N-alkylation, O-alkylation, and acylation reactions where strong inorganic bases cause side reactions. Provides clean product profiles with minimal elimination byproducts.

🔬 Pd-Catalyzed Reactions

Base of choice for palladium-catalyzed alkoxycarbonylation, Heck coupling, and Sonogashira reactions. Non-nucleophilic nature prevents catalyst poisoning and ensures high turnover numbers.

💊 Pharmaceutical Intermediates

Key reagent in the synthesis of antiviral agents (HIV protease inhibitors), oncology APIs, and CNS-targeted drug candidates. Used where trace amine contamination is unacceptable.